Combining the powers of electron diffraction, electron microscopy, PXRD and NMR for structure determination of complex disordered zeolites

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The Synthesis of Zeolites A, X and HS from Natural Iranian Kaolinite and the Study of the Transformation of Zeolites X to HS and Zeolites Y to P by X-ray diffraction and Scanning Electron Microscopy.

Zeolites A, X and HS were synthesized from natural Iranian Kaolinite by alkaline fusion,,followed by refluxing the mixture. The transformation of zeolites X to HS and Y to P were studied at different time intervals by X-ray diffraction and Scanning Electron Microscopy (SEM). It was revealed that in solution, zeolites HS and P are more stable than zeolites X and Y respectively

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Ab initio structure determination of interlayer expanded zeolites by single crystal rotation electron diffraction.

Layered solids often form thin plate-like crystals that are too small to be studied by single-crystal X-ray diffraction. Although powder X-ray diffraction (PXRD) is the conventional method for studying such solids, it has limitations because of peak broadening and peak overlapping. We have recently developed a software-based rotation electron diffraction (RED) method for automated collection an...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section A Foundations and Advances

سال: 2015

ISSN: 2053-2733

DOI: 10.1107/s205327331509289x